EXPERIMENTAL PROCEDURES FOR ASPIRIN
Calculating theoretical and experimental yield for Aspirin
Jul 19, 2012experimental procedure Part A.1. in the experiment, 2 g salicylic acid reacts with an excess amount of acetic anhydride Calculate the theoretical yield of acetylsalicylic acid (molar mass 180.2 g/mol) for this synthesis. after completing the experimental procedures, a mass of 1 of acetylsalicylic acid was recovered. what is the experimental yield for this synthesisStatus: Open
Wound healing activity of NOE-aspirin: A pre-clinical study
Esterification of aspirin. Acetylsalicylic acid (18 g, 0.1 m) was taken up in 50 ml of dry benzene and 24 ml of ethylene glycol to which was added 10 drops of p-toluene sulfonic acid. The mixture was heated under reflux with a Dean–Stark water separator for 11 h with periodic addition of dry benzene.Cited by: 9Publish Year: 2007Author: Mandeep Kaushal, N. Gopalan Kutty, C. Mallikarjuna Rao[PDF]
Traditional Undergraduate Experiment: Synthesis of Aspirin
An additional step may be added to the synthesis of aspirin: conversion of oil of wintergreen (methyl salicylate) to salicylic acid (Figure 2). This serves as an introduction to multi-step synthesis and the concept of converting a naturally occurring substance into one with therapeutic value.
Aspirin Lab Flashcards | Quizlet
Acetic anhydride when wet will react with the water molecules and form vinegar, and in our experiement we need the acetic anhydride to react with the salicyclic acid. The active ingredient, salicyclic acid, is found naturally in the leaves of willow trees.
Solved: Experimental Procedure, Part A.5. Recryslallizing
Experimental Procedure, Part A.5. Recryslallizing the aspirin removes some (or all) of the impurities in the sample. Explain how the recrystallization process performs this function. 3. Experimental Procedure, Part B.3. The melting point of the prepared aspirin in this experiment will most likely be less than (but not greater than) that of pure aspirin.100%(1)[PDF]
Aspirin Synthesis and Analysis - TCU Geology Department
• To prepare a sample of aspirin (organic synthesis). • Part B will NOT be performed. • The synthesis of aspirin is an esterification reaction. • Esterification is the general name for a chemical reaction in which two chemicals (typically an alcohol and an acid) form an ester as the reaction product (aspirin).[PDF]
Aspirin synthesis experimental - University of Calgary
SYNTHESIS OF ASPIRIN EXPERIMENTAL TECHNIQUES REQUIRED Recrystallisation (T 2), filtration (T 3), melting point determination (T 4), yield calculation (T 14) OTHER DOCUMENTS: Aspirin report EXPERIMENTAL PROCEDURE Acetic anhydride is toxic, corrosive and a lachrymator (causes tears) and a skin irritant. Avoid contact with skin, eyes and clothing.[PDF]
Experiment 5 - Synthesis of Aspirin
1 Aspirin is the common name for the compound acetylsalicylic acid, widely used as a fever reducer and as a pain killer. Salicylic acid, whose name comes from Salix, the willow family of plants, was derived from willow bark extracts. In folk medicine, willow bark teas were used as headache remedies and other tonics.
Synthesis of Aspirin: A General Chemistry Experiment
An experiment is described that is suitable for the early portion of the laboratory in a general chemistry course and integrates organic examples. It is the two-step synthesis of aspirin starting from oil of wintergreen. The mechanism for this synthesis provides examples of three major classes of chemical reactions: hydrolysis, condensation, and proton transfer.Published in: Journal of Chemical Education · 1998Authors: John OlmstedAbout: Salicylic acid · Chemical reaction · Curriculum development · Chemistry · Fourier tran[PDF]
Determination of Aspirin using Back Titration
Determination of Aspirin using Back Titration This experiment is designed to illustrate techniques used in a typical indirect or back titration. You will use the NaOH you standardized last week to back titrate an aspirin solution and determine the concentration of aspirin in a typical analgesic tablet. You will be graded on your accuracy
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